#### Experiments

 Crystal: Space group: P 4 (No. 75) Unit cell: $$\left( \begin{array}{cccccc} 57.784 & 57.784 & 150.001 & 90.000 & 90.000 & 90.000 \end{array}\right)$$ U matrix: $$\left( \begin{array}{rrr} 0.3455 & -0.2590 & -0.9020 \\ 0.8913 & 0.3911 & 0.2291 \\ 0.2934 & -0.8831 & 0.3660 \end{array} \right)$$ B matrix: $$\left( \begin{array}{rrr} 0.0173 & 0.0000 & 0.0000 \\ 0.0000 & 0.0173 & 0.0000 \\ -0.0000 & 0.0000 & 0.0067 \end{array} \right)$$ A = UB: $$\left( \begin{array}{rrr} 0.0060 & -0.0045 & -0.0060 \\ 0.0154 & 0.0068 & 0.0015 \\ 0.0051 & -0.0153 & 0.0024 \end{array} \right)$$ A sampled at 541 scan points Average unit cell: $$\left( \begin{array}{cccccc} 57.783 & 57.783 & 150.000 & 90.000 & 90.000 & 90.000 \end{array}\right)$$

#### Experimental geometry

 Panel 1: Pixel size (mm): 0.1720, 0.1720 Image size (pixels): 2463, 2527 Trusted range: -1, 161977 Thickness (mm): 0.32 Material: Si μ: 3.92203 Fast axis: $$\left( \begin{array}{rrr} 1.0000 & -0.0016 & -0.0016 \end{array} \right)$$ Slow axis: $$\left( \begin{array}{rrr} -0.0016 & -1.0000 & -0.0043 \end{array} \right)$$ Origin: $$\left( \begin{array}{rrr} -210.6683 & 205.7044 & -263.8433 \end{array} \right)$$ Distance (mm) 265.0648 Max resolution (corners) (Å): 1.16 Max resolution (inscribed circle) (Å): 1.51 Scan: Image range: 1, 540 Oscillation: 82, 0 Goniometer: Rotation axis: $$\left( \begin{array}{rrr} 1.0000 & 0.0000 & 0.0000 \end{array} \right)$$ Fixed rotation: $$\left( \begin{array}{rrr} 1.0000 & 0.0000 & 0.0000 \\ 0.0000 & 1.0000 & 0.0000 \\ 0.0000 & 0.0000 & 1.0000 \end{array} \right)$$ Setting rotation: $$\left( \begin{array}{rrr} 1.0000 & 0.0000 & 0.0000 \\ 0.0000 & 1.0000 & 0.0000 \\ 0.0000 & 0.0000 & 1.0000 \end{array} \right)$$